6L7S
Crystal structure of FKRP in complex with Mg ion, Zinc peak data
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-06 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.2825 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.939, 119.384, 257.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.300 - 2.410 |
R-factor | 0.1831 |
Rwork | 0.182 |
R-free | 0.21080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kan |
RMSD bond length | 0.007 |
RMSD bond angle | 0.782 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.300 | 2.450 |
High resolution limit [Å] | 2.410 | 2.410 |
Rmerge | 0.074 | 0.631 |
Rmeas | 0.088 | 0.695 |
Number of reflections | 177276 | 4418 |
<I/σ(I)> | 12.97 | 2.9 |
Completeness [%] | 100.0 | |
Redundancy | 3.4 | |
CC(1/2) | 0.998 | 0.839 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 4-8% PEG 4,000, 0.1 M HEPES-NaOH (pH7.5), and 0.2 M MgCl2 |