6L5H
Crystal structure of human rootletin 1108-1200
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-12-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 139.088, 32.162, 36.997 |
Unit cell angles | 90.00, 96.17, 90.00 |
Refinement procedure
Resolution | 22.087 - 1.300 |
R-factor | 0.1898 |
Rwork | 0.189 |
R-free | 0.20440 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AutoSol |
Refinement software | PHENIX (1.16-3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.320 |
High resolution limit [Å] | 1.300 | 3.530 | 1.300 |
Rmerge | 0.052 | 0.033 | 0.531 |
Rmeas | 0.056 | 0.036 | 0.581 |
Rpim | 0.021 | 0.014 | 0.231 |
Total number of observations | 281721 | ||
Number of reflections | 40235 | 2053 | 1999 |
<I/σ(I)> | 14.6 | ||
Completeness [%] | 99.8 | 97.2 | 98.4 |
Redundancy | 7 | 6.8 | 5.9 |
CC(1/2) | 0.999 | 0.940 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | 0.1 M HEPES pH 7.0, 14% PEG 4000 |