6L0Y
Structure of dsRNA with G-U wobble base pairs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-19 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97934 |
Spacegroup name | H 3 2 |
Unit cell lengths | 45.080, 45.080, 354.130 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.610 - 3.000 |
R-factor | 0.2374 |
Rwork | 0.232 |
R-free | 0.27910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 455d |
RMSD bond length | 0.002 |
RMSD bond angle | 0.412 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.610 | 3.107 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.043 | 0.099 |
Rmeas | 0.047 | 0.108 |
Rpim | 0.018 | 0.042 |
Number of reflections | 3067 | 280 |
<I/σ(I)> | 30.62 | 12.26 |
Completeness [%] | 98.7 | 99.29 |
Redundancy | 6.4 | 6.7 |
CC(1/2) | 1.000 | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30% PEG 4000, 0.2M Ammonium Sulfate |