6L0X
The First Tudor Domain of PHF20L1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 25.346, 32.019, 47.350 |
Unit cell angles | 84.99, 88.22, 82.84 |
Refinement procedure
Resolution | 25.317 - 1.300 |
R-factor | 0.154 |
Rwork | 0.152 |
R-free | 0.18180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sd4 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.928 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.320 | 1.350 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.049 | 0.363 |
Number of reflections | 29808 | 1817 |
<I/σ(I)> | 21.2 | |
Completeness [%] | 89.3 | |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 10% PEG 6000, 0.1M citric acid, PH 4.0 |