6KZY
Cu(II) loaded Tegillarca granosa ferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-12-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.73890 |
Spacegroup name | H 3 2 |
Unit cell lengths | 217.054, 217.054, 132.874 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.721 - 2.301 |
R-factor | 0.154153127908 |
Rwork | 0.152 |
R-free | 0.19456 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a9q |
RMSD bond length | 0.006 |
RMSD bond angle | 0.734 |
Data reduction software | xia2 |
Data scaling software | HKL-3000 |
Phasing software | BALBES |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.085 | 0.218 |
Number of reflections | 51876 | 2630 |
<I/σ(I)> | 32.604 | 21.456 |
Completeness [%] | 97.8 | 100 |
Redundancy | 8.6 | 8.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289.15 | 0.2M Ammonium acetate, 0.1M TRIS hydrochloride pH 7.5 |