6KVK
Crystal structure of UDP-Sm-SrUGT76G1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9798 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 98.013, 98.013, 89.529 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.051 - 2.397 |
R-factor | 0.2062 |
Rwork | 0.204 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vce |
RMSD bond length | 0.021 |
RMSD bond angle | 1.873 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.051 | 2.483 |
High resolution limit [Å] | 2.397 | 2.397 |
Rmeas | 0.142 | |
Number of reflections | 19809 | 1864 |
<I/σ(I)> | 22.5 | |
Completeness [%] | 100.0 | |
Redundancy | 19.2 | |
CC(1/2) | 0.986 | 0.803 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 24% (vol/vol) 2-propanol, 0.1 M sodium citrate tribasic dihydrate, pH 5.9, 20% (wt/vol) PEG4000 |