6KVJ
Crystal structure of UDPX-SrUGT76G1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9798 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 98.244, 98.244, 90.367 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.122 - 2.499 |
R-factor | 0.1834 |
Rwork | 0.181 |
R-free | 0.22950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vce |
RMSD bond length | 0.011 |
RMSD bond angle | 1.787 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.122 | 2.589 |
High resolution limit [Å] | 2.499 | 2.499 |
Rmeas | 0.134 | |
Number of reflections | 24046 | 1378 |
<I/σ(I)> | 16.5 | |
Completeness [%] | 100.0 | |
Redundancy | 8 | |
CC(1/2) | 0.998 | 0.716 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (vol/vol) 2-propanol, 0.1M sodium citrate tribasic dihydrate, pH 5.9, 20% (wt/vol) pEG4000 |