6KVI
Crystal structure of UDP-SrUGT76G1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9798 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 98.058, 98.058, 91.618 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.228 - 2.598 |
R-factor | 0.1941 |
Rwork | 0.191 |
R-free | 0.24890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vce |
RMSD bond length | 0.012 |
RMSD bond angle | 1.982 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.228 | 2.691 |
High resolution limit [Å] | 2.598 | 2.598 |
Rmeas | 0.147 | |
Number of reflections | 15678 | 1344 |
<I/σ(I)> | 12.2 | |
Completeness [%] | 99.3 | |
Redundancy | 6 | |
CC(1/2) | 0.785 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 18% (vol/vol) 2-propanol, 0.1 M sodium citrate tribasic dihydrate, pH 5.5, 20% (wt/vol) pEG4000 |