6KN5
Crystal structure of AFF4 C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2018-09-30 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97845 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 41.062, 71.117, 187.417 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.935 - 2.200 |
R-factor | 0.2518 |
Rwork | 0.247 |
R-free | 0.29230 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.719 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.940 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.069 | 0.946 |
Rmeas | 0.072 | |
Rpim | 0.020 | |
Number of reflections | 14447 | 1249 |
<I/σ(I)> | 21.8 | |
Completeness [%] | 100.0 | |
Redundancy | 12.8 | |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | sodium dihydrogen phosphate, potassium monohydrogen phosphate, 2-(N-morpholino)ethanesulfonic acid |