6KMH
The crystal structure of CASK/Mint1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-05-22 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 93.978, 96.321, 97.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.232 - 2.400 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.22410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tac |
RMSD bond length | 0.009 |
RMSD bond angle | 1.231 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.430 |
High resolution limit [Å] | 2.350 | 5.060 | 2.350 |
Rmerge | 0.121 | 0.071 | 0.518 |
Rmeas | 0.127 | 0.075 | 0.545 |
Rpim | 0.040 | 0.024 | 0.169 |
Total number of observations | 381609 | ||
Number of reflections | 37889 | 3990 | 3725 |
<I/σ(I)> | 12.1 | ||
Completeness [%] | 99.9 | 99.3 | 100 |
Redundancy | 10.1 | 9.6 | 10.2 |
CC(1/2) | 0.997 | 0.972 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M KI, 20% PEG 3350, pH 7.0 |