6KJX

Galectin-13 variant C138S

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-21
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.00000
Spacegroup name	P 43 21 2
Unit cell lengths	53.617, 53.617, 113.810
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.515 - 1.530
R-factor	0.1849
Rwork	0.183
R-free	0.20870
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.159
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.520	1.560
High resolution limit [Å]	1.530	1.530
Number of reflections	25914	1255
<I/σ(I)>	25.2
Completeness [%]	99.9
Redundancy	9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Bis-Tris