6KJX
Galectin-13 variant C138S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 53.617, 53.617, 113.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.515 - 1.530 |
R-factor | 0.1849 |
Rwork | 0.183 |
R-free | 0.20870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.159 |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.520 | 1.560 |
High resolution limit [Å] | 1.530 | 1.530 |
Number of reflections | 25914 | 1255 |
<I/σ(I)> | 25.2 | |
Completeness [%] | 99.9 | |
Redundancy | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | Bis-Tris |