6KIT

Structure of mouse CXorf40A, Selenomethionine derivative

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-08
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97623
Spacegroup name	P 21 21 2
Unit cell lengths	51.128, 96.102, 33.230
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.570
R-factor	0.1851
Rwork	0.183
R-free	0.21740
Structure solution method	SAD
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	SHELXDE
Refinement software	REFMAC (5)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.630
High resolution limit [Å]	1.570	1.570
Number of reflections	23707	2320
<I/σ(I)>	22.21
Completeness [%]	100.0
Redundancy	12.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M HEPES sodium pH 7.5, 2% v/v Polyethylene glycol 400, 2.0 M Ammonium sulfate