6KIH
Sucrose-phosphate synthase (tll1590) from Thermosynechococcus elongatus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-12-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 116.662, 170.835, 160.546 |
| Unit cell angles | 90.00, 96.43, 90.00 |
Refinement procedure
| Resolution | 19.900 - 3.000 |
| R-factor | 0.268 |
| Rwork | 0.266 |
| R-free | 0.27760 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3c4q |
| Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.900 | 3.060 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.119 | 0.855 |
| Number of reflections | 122717 | 5683 |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 98.7 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | PEG |
