6KIH
Sucrose-phosphate synthase (tll1590) from Thermosynechococcus elongatus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 116.662, 170.835, 160.546 |
Unit cell angles | 90.00, 96.43, 90.00 |
Refinement procedure
Resolution | 19.900 - 3.000 |
R-factor | 0.268 |
Rwork | 0.266 |
R-free | 0.27760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c4q |
Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.900 | 3.060 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.119 | 0.855 |
Number of reflections | 122717 | 5683 |
<I/σ(I)> | 7.6 | |
Completeness [%] | 98.7 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | PEG |