6KHO
Crystal structure of Oryza sativa TDC with PLP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NFPSS BEAMLINE BL19U1 |
Synchrotron site | NFPSS |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-30 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.97915 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 155.733, 155.733, 102.182 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.717 - 1.972 |
R-factor | 0.1699 |
Rwork | 0.169 |
R-free | 0.19450 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.030 |
High resolution limit [Å] | 1.970 | 1.970 |
Rmerge | 0.083 | 0.625 |
Number of reflections | 98063 | 9359 |
<I/σ(I)> | 39.6 | 2.476 |
Completeness [%] | 97.5 | 93.6 |
Redundancy | 9.3 | 9.3 |
CC(1/2) | 0.844 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | PEG 1000, Imidazole/Hydrochloric acid, Calcium acetate |