6KF8
OsACBP2 in complex with C18:3-CoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-11-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97894 |
Spacegroup name | H 3 |
Unit cell lengths | 149.965, 149.965, 95.443 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.830 - 3.600 |
R-factor | 0.2299 |
Rwork | 0.228 |
R-free | 0.27920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5h3i |
RMSD bond length | 0.008 |
RMSD bond angle | 1.411 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.910 | 3.700 |
High resolution limit [Å] | 3.510 | 3.510 |
Rmerge | 0.136 | 0.522 |
Number of reflections | 9948 | 1445 |
<I/σ(I)> | 6.8 | |
Completeness [%] | 99.5 | |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1M MES pH 6.5, 30% PEG 4000 |