6K9N
Rice_OTUB_like_catalytic domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-11-22 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9873 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.688, 144.810, 155.848 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.380 - 2.270 |
R-factor | 0.1879 |
Rwork | 0.186 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zfy |
RMSD bond length | 0.004 |
RMSD bond angle | 0.717 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.290 |
High resolution limit [Å] | 2.250 | 2.250 |
Rpim | 0.035 | 0.158 |
Number of reflections | 62083 | 3018 |
<I/σ(I)> | 7.54 | |
Completeness [%] | 99.7 | |
Redundancy | 10.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 291 | 0.15 M Potassium bromide, 30% w/v Polyethylene glycol monomethyl ether 2,000 |