6K90
Pyridoxal Kinase from Leishmania donovani in complex with ADP and Pyridoxamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-05-17 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.550, 71.410, 76.880 |
Unit cell angles | 90.00, 99.07, 90.00 |
Refinement procedure
Resolution | 35.570 - 1.900 |
R-factor | 0.17597 |
Rwork | 0.174 |
R-free | 0.20995 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.637 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.700 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 44075 | 2767 |
<I/σ(I)> | 18.3 | |
Completeness [%] | 96.0 | |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 16% PEG 8000, 0.1M Sodium Cacodylate, 0.32M Calcium Acetate, 6% Glycerol |