6K8A
RGLG1 VWA domain with MIDAS is occupied by water
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AichiSR BEAMLINE BL2S1 |
Synchrotron site | AichiSR |
Beamline | BL2S1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-12-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.978897 |
Spacegroup name | P 41 |
Unit cell lengths | 136.280, 136.280, 55.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.009 - 2.400 |
R-factor | 0.1791 |
Rwork | 0.177 |
R-free | 0.21070 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.180 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.010 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.217 | 1.780 |
Number of reflections | 39684 | 2909 |
<I/σ(I)> | 2 | |
Completeness [%] | 98.9 | 99.4 |
Redundancy | 13.5 | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M magnesium chloride, 0.1 M sodium citrate ph 6.5, 5%(w/v) MPD |