6K89
The closed state of RGLG1 VWA domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AichiSR BEAMLINE BL2S1 |
Synchrotron site | AichiSR |
Beamline | BL2S1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-09-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.978897 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.619, 72.935, 80.077 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.038 - 1.689 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.23070 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.036 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.610 | 1.700 |
Rmerge | 0.143 | 0.067 | 1.412 |
Rmeas | 0.149 | 0.070 | 1.504 |
Rpim | 0.042 | 0.020 | 0.507 |
Total number of observations | 367235 | ||
Number of reflections | 30477 | 1682 | 1463 |
<I/σ(I)> | 2.5 | ||
Completeness [%] | 99.7 | 99.8 | 99.3 |
Redundancy | 12 | 11.9 | 8.3 |
CC(1/2) | 0.997 | 0.476 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M NaAc, 25%PEG4K, 8% isopropanol |