6K87
The closed state of RGLG1 VWA domain with MIDAS is occupied by water
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AichiSR BEAMLINE BL2S1 |
Synchrotron site | AichiSR |
Beamline | BL2S1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-09-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.978897 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.789, 73.690, 82.436 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.978 - 1.502 |
R-factor | 0.1943 |
Rwork | 0.193 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.045 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.530 |
High resolution limit [Å] | 1.500 | 4.070 | 1.500 |
Rmerge | 0.189 | 0.120 | 0.949 |
Rmeas | 0.201 | 0.128 | 1.027 |
Rpim | 0.067 | 0.043 | 0.371 |
Total number of observations | 313357 | ||
Number of reflections | 39569 | 2177 | 1504 |
<I/σ(I)> | 3.5 | ||
Completeness [%] | 93.6 | 94 | 72.9 |
Redundancy | 7.9 | 8.1 | 6.2 |
CC(1/2) | 0.986 | 0.259 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 50 mM LiSO4, 50 mM NaSO4, 0.1 M Mes ph 6.5, 30%PEG8k |