6K4J
Crystal Structure of the the CD9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-21 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 45.180, 125.210, 129.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.498 - 2.701 |
R-factor | 0.2647 |
Rwork | 0.262 |
R-free | 0.28890 |
Structure solution method | SIRAS |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.498 | 42.498 | 2.860 |
High resolution limit [Å] | 2.700 | 8.080 | 2.700 |
Rmerge | 0.051 | 0.097 | 3.135 |
Rmeas | 0.518 | 0.098 | 3.162 |
Total number of observations | 604284 | ||
Number of reflections | 10431 | 438 | 1623 |
<I/σ(I)> | 15.83 | 65.52 | 1.7 |
Completeness [%] | 100.0 | 99.1 | 100 |
Redundancy | 57.932 | 57.135 | 59.792 |
CC(1/2) | 0.998 | 0.999 | 0.513 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 6.5 | 298 | PEG 200 |