6K4E
SiaA-PP2C domain of Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2019-02-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9764 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.170, 110.480, 111.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.810 - 2.094 |
R-factor | 0.213 |
Rwork | 0.212 |
R-free | 0.24100 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.060 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AutoSol |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.810 | 2.169 |
High resolution limit [Å] | 2.094 | 2.094 |
Rmerge | 0.160 | 1.432 |
Rpim | 0.076 | 0.663 |
Number of reflections | 37739 | 3471 |
<I/σ(I)> | 7.2 | |
Completeness [%] | 99.2 | |
Redundancy | 5.5 | |
CC(1/2) | 0.993 | 0.461 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | Morpheus A11 from Molecular Dimensions |