6K2Y

Human Galectin-14

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-19
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.98
Spacegroup name	P 21 21 21
Unit cell lengths	35.629, 63.223, 130.936
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.609 - 1.570
R-factor	0.2128
Rwork	0.211
R-free	0.24120
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.170	1.600
High resolution limit [Å]	1.570	1.570
Number of reflections	42281	2067
<I/σ(I)>	22.4
Completeness [%]	99.9
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG