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6K2L

Crystal structure of the Siderophore-interacting protein SipS from Aeromonas hydrophila

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 5C (4A)
Synchrotron sitePAL/PLS
Beamline5C (4A)
Temperature [K]100
Detector technologyCCD
Collection date2018-10-12
DetectorADSC QUANTUM 315r
Wavelength(s)0.979463
Spacegroup nameC 2 2 21
Unit cell lengths130.402, 149.991, 55.896
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution36.933 - 2.500
R-factor0.2076
Rwork0.203
R-free0.26050
Structure solution methodSAD
RMSD bond length0.009
RMSD bond angle1.071
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX ((1.15.2_3472: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.390
High resolution limit [Å]2.3502.350
Number of reflections24604176
<I/σ(I)>14.5962.386
Completeness [%]99.397.7
Redundancy9.25.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52870.18 M Lithium sulfate monohydrate, 30% (w/v) Polyethylene glycol 4,000 and 0.1 M Tris hydrochloride, pH 8.5

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