6K2E
Crystal structure of cas2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2019-05-14 |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.54 |
Spacegroup name | P 62 |
Unit cell lengths | 101.313, 101.313, 39.585 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.420 - 2.800 |
R-factor | 0.2138 |
Rwork | 0.208 |
R-free | 0.26820 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5g4d |
RMSD bond length | 0.011 |
RMSD bond angle | 1.252 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.14_3260) |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.420 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 5885 | 587 |
<I/σ(I)> | 12 | |
Completeness [%] | 99.7 | |
Redundancy | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 280 | 0.02M Magnesium, 16.5% v/v 2-propanol, 0.1M Sodium Cacodylate pH 6.6 |