6K0C

Crystal structure of ceNAP1-H2A.Z-H2B complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-15
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9789
Spacegroup name	P 21 21 21
Unit cell lengths	67.728, 79.313, 174.329
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.394 - 2.281
R-factor	0.2187
Rwork	0.217
R-free	0.26230
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.394	2.360
High resolution limit [Å]	2.280	2.280
Rmerge		0.642
Number of reflections	43537	43537
<I/σ(I)>	14.43
Completeness [%]	99.9
Redundancy	6.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	20% PEG 3350