6K03
Crystal structure of ceH2A-H2B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-18 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 63.839, 63.839, 70.032 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.394 - 2.857 |
R-factor | 0.2366 |
Rwork | 0.231 |
R-free | 0.28370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6k01 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.390 | 2.960 |
High resolution limit [Å] | 2.857 | 2.857 |
Rmerge | 0.680 | |
Number of reflections | 3967 | 3967 |
<I/σ(I)> | 12.15 | |
Completeness [%] | 97.5 | |
Redundancy | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20% PEG3350 |