6K00
Crystal structure A of ceNAP1-H2A-H2B complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9790 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.298, 78.724, 169.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.351 - 2.198 |
R-factor | 0.2123 |
Rwork | 0.211 |
R-free | 0.24260 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.351 | 2.280 |
High resolution limit [Å] | 2.198 | 2.198 |
Rmerge | 0.827 | |
Number of reflections | 46721 | 46721 |
<I/σ(I)> | 17.74 | |
Completeness [%] | 99.9 | |
Redundancy | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20% PEG8000 |