6JZV
Crystal structure of SufU from Bacillus subtilis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.25865 |
Spacegroup name | P 1 |
Unit cell lengths | 35.320, 54.450, 70.380 |
Unit cell angles | 68.99, 75.86, 72.54 |
Refinement procedure
Resolution | 49.409 - 2.000 |
R-factor | 0.213 |
Rwork | 0.211 |
R-free | 0.24170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xt5 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.409 | 49.409 | 2.100 |
High resolution limit [Å] | 2.000 | 10.000 | 2.000 |
Rmerge | 0.187 | 0.146 | 0.931 |
Rmeas | 0.201 | 0.154 | 0.999 |
Total number of observations | 499479 | ||
Number of reflections | 31156 | 496 | 8493 |
<I/σ(I)> | 8.64 | 19.17 | 2.65 |
Completeness [%] | 99.5 | 97.3 | 99.7 |
Redundancy | 8.033 | 8.651 | 8.105 |
CC(1/2) | 0.993 | 0.995 | 0.712 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 0.15 M potassium thiocyanate, 0.1M MES, 20% w/v PEG1500 |