6JZN
Structure of the intermembrane space region of PARC6-PDV1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 91.454, 95.827, 196.566 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.142 - 2.894 |
R-factor | 0.2251 |
Rwork | 0.223 |
R-free | 0.27150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6jzf |
RMSD bond length | 0.007 |
RMSD bond angle | 1.260 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.142 | 2.997 |
High resolution limit [Å] | 2.890 | 2.894 |
Number of reflections | 18678 | 1302 |
<I/σ(I)> | 11.28 | |
Completeness [%] | 95.0 | |
Redundancy | 7.1 | |
CC(1/2) | 0.997 | 0.904 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | sodium acetate, phosphate potassium |