6JYX
Structure of CbpJ from Streptococcus Pneumoniae TIGR4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-07 |
Detector | MARRESEARCH |
Wavelength(s) | 0.97923 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.523, 77.378, 187.848 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.680 - 2.000 |
R-factor | 0.21603 |
Rwork | 0.214 |
R-free | 0.25603 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v04 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.289 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.072 | 0.199 |
Number of reflections | 51107 | 1000 |
<I/σ(I)> | 10.259 | |
Completeness [%] | 93.4 | |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 10% PEG 20K, 0.1 M MES pH 6.5 |