6JYR
GII.13/21 noroviruses recognize glycans with a terminal beta-galactose via an unconventional glycan binding site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 113 |
Detector technology | PIXEL |
Collection date | 2018-06-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97917 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.142, 107.512, 99.538 |
Unit cell angles | 90.00, 98.31, 90.00 |
Refinement procedure
Resolution | 40.959 - 1.501 |
R-factor | 0.1784 |
Rwork | 0.178 |
R-free | 0.19280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.713 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 197138 | |
<I/σ(I)> | 25.444 | |
Completeness [%] | 98.9 | |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291 | 0.2 M ammonium acetate, 0.1 M HEPES pH 7.5, 25% polyethylene glycol 3350 |