6JY4
Monomeric Form of Bovine Heart Cytochrome c Oxidase in the Fully Reduced State
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 50 |
Detector technology | CCD |
Collection date | 2011-07-27 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 149.395, 152.395, 174.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.950 |
R-factor | 0.15492 |
Rwork | 0.152 |
R-free | 0.20454 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5b1b |
RMSD bond length | 0.020 |
RMSD bond angle | 1.938 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 200.000 | 1.920 |
High resolution limit [Å] | 1.900 | 1.900 |
Rpim | 0.032 | 0.373 |
Number of reflections | 278336 | 9391 |
<I/σ(I)> | 28.2 | 2.2 |
Completeness [%] | 89.5 | |
Redundancy | 9 | |
CC(1/2) | 0.734 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 277 | sodium phosphate, PEG 4000, DM |