6JWF
Holo form of Pyranose Dehydrogenase PQQ domain from Coprinopsis cinerea
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-27 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.330, 95.638, 106.204 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.070 - 1.300 |
R-factor | 0.16 |
Rwork | 0.160 |
R-free | 0.17700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6jt5 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.380 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.067 | 0.543 |
Number of reflections | 213104 | 33130 |
<I/σ(I)> | 15 | 2.99 |
Completeness [%] | 99.4 | 96.3 |
Redundancy | 7.4 | 7.2 |
CC(1/2) | 0.999 | 0.863 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 5 | 277 | 5mM sodium acetate |