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6JU0

Mouse antibody 3.3 Fab in complex with PEG

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL12B2
Synchrotron siteSPring-8
BeamlineBL12B2
Temperature [K]100
Detector technologyCCD
Collection date2013-09-15
DetectorADSC QUANTUM 210
Wavelength(s)1.0000
Spacegroup nameP 1 21 1
Unit cell lengths69.299, 177.347, 89.019
Unit cell angles90.00, 91.99, 90.00
Refinement procedure
Resolution24.503 - 2.601
R-factor0.2117
Rwork0.211
R-free0.24010
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3w9d
RMSD bond length0.002
RMSD bond angle0.686
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0002.690
High resolution limit [Å]2.6002.600
Rpim0.0520.361
Number of reflections644346420
<I/σ(I)>15.12.2
Completeness [%]98.698.5
Redundancy3.13
CC(1/2)0.9280.699
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.6291PEG 4000, 2-propanol, PEG 2000 MME, Ni-citrate

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