6JTQ
RVD HA specifically contacts 5mC through van der Waals interactions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-06-20 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.786, 88.022, 89.349 |
Unit cell angles | 90.00, 104.77, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.480 |
R-factor | 0.22107 |
Rwork | 0.218 |
R-free | 0.28338 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.813 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.547 |
High resolution limit [Å] | 2.480 | 2.480 |
Number of reflections | 39755 | |
<I/σ(I)> | 2.03 | |
Completeness [%] | 98.8 | |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 8-10% PEG3350 (w/v), 10% ethanol, 0.1 M MES pH 6.7 |