6JTD

Crystal structure of TcCGT1 in complex with UDP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-04
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97930
Spacegroup name	P 1 21 1
Unit cell lengths	56.304, 108.702, 90.432
Unit cell angles	90.00, 106.17, 90.00

Refinement procedure

Resolution	39.682 - 1.850
R-factor	0.1707
Rwork	0.169
R-free	0.19740
RMSD bond length	0.012
RMSD bond angle	1.205
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.900
High resolution limit [Å]	1.850	1.850
Number of reflections	88344
<I/σ(I)>	11.6	2
Completeness [%]	98.9	97.9
Redundancy	3.4	3.2
CC(1/2)	0.981	0.696

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1M potassium chloride, 0.02M Tris 7.0, 20% w/v PEG 4000