6JR5
ZHD/H242A complex with bZOL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97916 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.610, 91.680, 113.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.000 - 2.080 |
R-factor | 0.1913 |
Rwork | 0.189 |
R-free | 0.23508 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5c8z |
RMSD bond length | 0.009 |
RMSD bond angle | 1.489 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 113.640 | 2.130 |
High resolution limit [Å] | 2.080 | 2.080 |
Rmerge | 0.103 | 0.627 |
Rpim | 0.063 | 0.370 |
Number of reflections | 47254 | 3470 |
<I/σ(I)> | 12.2 | |
Completeness [%] | 99.2 | |
Redundancy | 6.9 | |
CC(1/2) | 0.997 | 0.866 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | ammonium phosphate, imidazole, potassium chloride |