6JO7
Crystal structure of mouse MXRA8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-08-02 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97894 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 72.446, 143.486, 196.346 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.341 - 2.400 |
R-factor | 0.22 |
Rwork | 0.219 |
R-free | 0.24460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tt3 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.606 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 40460 | 3978 |
<I/σ(I)> | 22.1 | 1.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 | 12.3 |
CC(1/2) | 0.997 | 0.691 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 0.1 M BICINE pH 8.5, 15% w/v Polyethylene glycol 1500 |