6JMG
Crystal structure of xRbj
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97910 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 107.630, 107.630, 320.247 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.701 |
R-factor | 0.2108 |
Rwork | 0.208 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.183 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 31168 | |
<I/σ(I)> | 30.1 | |
Completeness [%] | 99.9 | |
Redundancy | 19.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1M Bis-Tris pH 6.5, 28% (w/v) Polyethylene glycol monomethyl ether 2000 |