6JJB

BRD4 in complex with ZZM1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-26
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9793
Spacegroup name	P 21 21 21
Unit cell lengths	32.480, 47.070, 78.660
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	26.730 - 1.508
R-factor	0.1974
Rwork	0.194
R-free	0.22780
Data reduction software	TRUNCATE
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3235)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	26.730	1.562
High resolution limit [Å]	1.508	1.508
Number of reflections	19301
<I/σ(I)>	116.02
Completeness [%]	95.4
Redundancy	33.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	4.0M HCOONa