6JJ5
BRD4 in complex with 259
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-26 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.060, 47.200, 79.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.535 - 1.200 |
R-factor | 0.1773 |
Rwork | 0.176 |
R-free | 0.20260 |
Data reduction software | TRUNCATE |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3235) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.535 | 1.243 |
High resolution limit [Å] | 1.200 | 1.200 |
Number of reflections | 38139 | |
<I/σ(I)> | 8.71 | |
Completeness [%] | 99.4 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 4.0M HCOONa |