6JJ3

BRD4 in complex with 138A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-26
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9793
Spacegroup name	P 21 21 21
Unit cell lengths	32.666, 46.918, 78.270
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.242 - 1.718
R-factor	0.2385
Rwork	0.235
R-free	0.30470
Data reduction software	TRUNCATE
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3235)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.242	1.779
High resolution limit [Å]	1.718	1.718
Number of reflections	12609
<I/σ(I)>	9.24
Completeness [%]	93.9
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	4.0M HCOONa