6JHZ
Crystal structure of cas2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-11-23 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 26.592, 76.391, 88.445 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.746 - 1.999 |
R-factor | 0.1979 |
Rwork | 0.195 |
R-free | 0.23220 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.861 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MoRDa |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.746 | 2.070 |
High resolution limit [Å] | 1.999 | 1.999 |
Number of reflections | 13958 | |
<I/σ(I)> | 13.5 | |
Completeness [%] | 99.2 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 280 | 0.1M Tris, pH8.5, 2M Ammonium sulfate |