6JHE
Crystal Structure of Bacillus subtilis SigW domain 4 in complexed with -35 element DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-08-05 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97933 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 61.620, 61.620, 119.971 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.842 - 3.101 |
R-factor | 0.2496 |
Rwork | 0.247 |
R-free | 0.28950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h27 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3051) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.104 | 0.524 |
Number of reflections | 3013 | 468 |
<I/σ(I)> | 62.8 | |
Completeness [%] | 99.4 | 100 |
Redundancy | 15.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 6.5 | 293 | PEG 1500, isopropanol, CaCl2 |