6JH5
Structure of Marine bacterial laminarinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2018-11-17 |
Detector | DECTRIS PILATUS3 X 2M |
Wavelength(s) | 1.000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 66.775, 101.879, 75.529 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.850 - 1.540 |
R-factor | 0.15091 |
Rwork | 0.150 |
R-free | 0.17462 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4crq |
RMSD bond length | 0.021 |
RMSD bond angle | 1.824 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.850 | 1.560 |
High resolution limit [Å] | 1.540 | 1.540 |
Rmerge | 0.032 | 0.266 |
Number of reflections | 34923 | 739 |
<I/σ(I)> | 32.3 | 2.8 |
Completeness [%] | 90.4 | 39.2 |
Redundancy | 5.9 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 15% (v/v) ethonal, 100 mM MES pH7.0 |