6JAK
OtsA apo structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-27 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.470, 119.660, 99.430 |
Unit cell angles | 90.00, 91.88, 90.00 |
Refinement procedure
Resolution | 29.687 - 2.410 |
R-factor | 0.1828 |
Rwork | 0.180 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1uqu |
RMSD bond length | 0.014 |
RMSD bond angle | 1.493 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.420 | 2.470 |
High resolution limit [Å] | 2.410 | 2.410 |
Rmerge | 0.134 | 0.800 |
Rpim | 0.080 | 0.521 |
Number of reflections | 75262 | 7695 |
<I/σ(I)> | 8.2 | 2.1 |
Completeness [%] | 95.3 | |
Redundancy | 7.2 | |
CC(1/2) | 0.993 | 0.685 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 0.1M Tris pH 8.5, 25% PEG 3350 |