6J9M
NmeBH+AcrIIC2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2017-12-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.385, 81.996, 76.063 |
Unit cell angles | 90.00, 96.44, 90.00 |
Refinement procedure
Resolution | 41.475 - 2.394 |
R-factor | 0.1817 |
Rwork | 0.179 |
R-free | 0.22230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6j9k |
RMSD bond length | 0.006 |
RMSD bond angle | 1.185 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.430 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.097 | 0.274 |
Number of reflections | 22256 | 1113 |
<I/σ(I)> | 29.6 | |
Completeness [%] | 99.8 | |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M CHES, ethanol |