6J9L
FnoBH+AcrIIC2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 193 |
| Detector technology | PIXEL |
| Collection date | 2017-12-04 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9785 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 49.706, 62.525, 88.812 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.410 - 1.780 |
| R-factor | 0.1795 |
| Rwork | 0.177 |
| R-free | 0.22392 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6j9k |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.923 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.810 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Rmerge | 0.088 | 0.398 |
| Number of reflections | 27092 | 1281 |
| <I/σ(I)> | 26.4 | |
| Completeness [%] | 99.6 | |
| Redundancy | 12.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M MES, pH 5.6, PEG 3000, PEG 200 |
