6J7Y
Human mitochondrial Oligoribonuclease in complex with DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL15A1 |
Synchrotron site | NSRRC |
Beamline | BL15A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-29 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 87.282, 125.293, 85.478 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.340 - 2.203 |
R-factor | 0.2021 |
Rwork | 0.198 |
R-free | 0.24380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2igi |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.240 |
High resolution limit [Å] | 2.200 | 5.970 | 2.200 |
Rmerge | 0.079 | 0.029 | 0.565 |
Number of reflections | 23925 | 1292 | 1172 |
<I/σ(I)> | 13.7 | ||
Completeness [%] | 99.3 | 98.5 | 98.6 |
Redundancy | 6.7 | 6.2 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298.15 | 0.2 M Ammonium citrate dibasic, 20% w/v PEG 3350 |